HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 12931834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | (1-Ethoxycyclopropoxy)trimethylsilane | HCID 2734686 | — |
| Product | HCID 12931834 | HCID 12931834 | 52% |
Reaction Steps
The reaction of (1-ethoxycyclopropoxy)trimethylsilane 13 and piperidine 14A with trimethylsilylcyanide yielded 1-(piperidin-1-yl)cyclopropanecarbonitrile as a yellow liquid (52%). MS ISP (m/e): 151.1 (68) [(M+H)]+, 149.2 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802665B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-faee700d5ce04444921eb7a87e714ecb |
| Source note | uspto-grants-2014_08 |