HRID2403157

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID296716

Methyl 2,4-dibromobutanoate

C5H8Br2O2

HCID23150669

4,4-Difluorocyclohexan-1-amine--hydrogen chloride (1/1)

C6H12ClF2N

PRODUCTS

生成物

HCID86692750

未命名化合物

收率 30%

PROCEDURE

实验过程

The reaction of methyl 2,4-dibromobutanoate 17 with 4,4-difluorocyclohexylamine hydrochloride 18B yielded methyl 1-(4,4-difluorocyclohexyl)azetidine-2-carboxylate as a brown oil (30%). MS ISP (m/e): 234.1 (100) [(M+H)]+.