HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,4-dibromobutanoate → HCID 86692754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,4-dibromobutanoate | HCID 296716 | — |
| Reactant | 2,2-dimethyltetrahydro-2H-pyran-4-amine | HCID 3809203 | — |
| Product | HCID 86692754 | HCID 86692754 | 33% |
Reaction Steps
The reaction of methyl 2,4-dibromobutanoate 17 with 2,2-dimethyltetrahydro-2H-pyran-4-amine 18H yielded methyl 1-(2,2-dimethyltetrahydro-2H-pyran-4-yl)azetidine-2-carboxylate as a light brown solid (33%). MS ISP (m/e): 228.3 (100) [(M+H)]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802665B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-c70271c1f3724241a696d6ded8706bea |
| Source note | uspto-grants-2014_08 |