HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,4-dibromobutanoate → HCID 86692755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,4-dibromobutanoate | HCID 296716 | — |
| Reactant | Tetrahydrothiopyran-4-ylamine | HCID 418807 | — |
| Product | HCID 86692755 | HCID 86692755 | 35% |
Reaction Steps
The reaction of methyl 2,4-dibromobutanoate 17 with tetrahydro-thiopyran-4-ylamine 18J yielded methyl 1-(tetrahydro-2H-thiopyran-4-yl)azetidine-2-carboxylate as a light brown solid (35%). MS ISP (m/e): 216.3 (100) [(M+H)]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802665B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-ce0b897f55774c4b8716decd2d1b9f8e |
| Source note | uspto-grants-2014_08 |