HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86675734, compound → HCID 86675733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86675734 | HCID 86675734 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86675733 | HCID 86675733 | 57% |
Reaction Steps
A solution of 98 (38 mg) in MeOH (10 ml) was stirred for 1 h under hydrogen atmosphere in the presence of 10% Pd/C. The resulting mixture was filtered through celite and the filtrate was evaporated under reduced pressure to give 181 as white solid (16 mg, 57%). ESI-MS m/z: 268.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802666B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-9dcabe7a0b7f463fba153648514f26be |
| Source note | uspto-grants-2014_08 |