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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2403248Generated: October 31, 2026

HCID 86675734, compound → HCID 86675733, compound

https://huagongshe.com/reaction/2403248

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86675734HCID 86675734—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 86675733HCID 8667573357%

Reaction Steps

A solution of 98 (38 mg) in MeOH (10 ml) was stirred for 1 h under hydrogen atmosphere in the presence of 10% Pd/C. The resulting mixture was filtered through celite and the filtrate was evaporated under reduced pressure to give 181 as white solid (16 mg, 57%). ESI-MS m/z: 268.1 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08802666B2
Source datasetuspto-grants-2014_08
ORD IDord-9dcabe7a0b7f463fba153648514f26be
Source noteuspto-grants-2014_08