HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5-nitropicolinate → HCID 67151276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5-nitropicolinate | HCID 12457882 | — |
| Solvent | Piperidine | HCID 8082 | — |
| Product | HCID 67151276 | HCID 67151276 | — |
Reaction Steps
Methyl 5-nitropyridine-2-carboxylate (182 g, 1 mol) was refluxed in piperidine (250 mL) for 1 hour. The reaction mixture was concentrated in vacuo to give crude 5-nitro-2-(piperidin-1-ylcarbonyl)pyridine, which was used for the next stage without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802690B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-7189845501844ad99b93ddd3866f2d67 |
| Source note | uspto-grants-2014_08 |