Diethanolamine → HCID 60686373, compound

HRID 2404305Notes

Reaction equation

HRID 2404305 reaction equation
Br[CH2:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[C:6]#[N:7].[NH:11]([CH2:15][CH2:16][OH:17])[CH2:12][CH2:13][OH:14]>>[OH:14][CH2:13][CH2:12][N:11]([CH2:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[C:6]#[N:7])[CH2:15][CH2:16][OH:17]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 97249Benzonitrile, 3-(bromomethyl)-

Product 1

HCID 60686373HCID 60686373, compound

Procedure

The title compound was prepared following the general procedure 10, starting from 3-(bromomethyl)benzonitrile and diethanolamine. It was obtained as a colorless oil (820 mg, 73%). LC/MS (Method B): 219.1 (M−H)−, 221.1 (M+H)+.

Sources & evidence

ORD record
ord-679d73e0031a45d298498755fb8bfc97
Source dataset
uspto-grants-2014_08
Patent number
US08802704B2

Reaction notes

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