HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)benzonitrile → HCID 66677749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Reactant | tert-butyl 4-(methylamino)butanoate hydrochloride | HCID 50988532 | — |
| Product | HCID 66677749 | HCID 66677749 | — |
Reaction Steps
The title compound was prepared following general procedure 10, starting from 4-cyanobenzyl bromide and tert-butyl 4-(methylamino)butanoate hydrochloride (Watanabe). It was obtained as a yellow oil (586 mg, quantitative). LC/MS (Method B): 289.2 (M+H)+. HPLC (Method A) Rt 3.02 (Purity: 91.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802704B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-6b65213db08f465892d487607097486e |
| Source note | uspto-grants-2014_08 |