HuagongsheHuagongshe Chemistry Print Report · For research reference only
Barium permanganate → HCID 44427556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Barium permanganate | HCID 24587 | — |
| Reactant | HCID 66835939 | HCID 66835939 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 44427556 | HCID 44427556 | — |
Reaction Steps
A mixture benzothiazol-2-yl(3-propoxyphenyl)methanol (1 g) and barium permanganate (0.95 g) in acetonitrile 15 mL) is refluxed for 30 minutes. The mixture is filtered over a clarcel pad, concentrated under reduced pressure and purified by column chromatography over silica gel (eluant heptane/ethyl acetate: 4/1) to give benzothiazol-2-yl(3-propoxyphenyl)methanone as a white cristalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802664B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-ba2397e138be4ebeb6363fbb8ee24ea5 |
| Source note | uspto-grants-2014_08 |