HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68486741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 42629164 | HCID 42629164 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68486741 | HCID 68486741 | 99.8% |
Reaction Steps
9.2 g of 2-fluoro-4-methyl-5-mercaptoaniline disclosed in WO2006/043635 was dissolved in 70 mL of water, and 9.7 g of potassium carbonate and 8.3 g of iodomethane were added under cooling with ice, followed by stirring at room temperature for 2 hours. The formed crystals were collected by filtration and washed with water to obtain 10.0 g of 2-fluoro-4-methyl-5-methylthioaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802713B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-a07b3167e0fc4e0aa5901c82c7456103 |
| Source note | uspto-grants-2014_08 |