HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamide → HCID 178518064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamide | HCID 713 | — |
| Reactant | Ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate | HCID 78262 | — |
| Product | HCID 178518064 | HCID 178518064 | — |
Reaction Steps
A solution of 10 millimol IV in 15 milliliter formamide was stirred at 100° C. for 3 hours then cooled down to room temperature. The reaction mixture was poured onto crushed ice with continuous stirring then collected by filtration. The product was washed with water and n-hexane, then dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802849B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-f0bb1876f5634d4286cc669c9e7cfd02 |
| Source note | uspto-grants-2014_08 |