HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2404945Generated: October 30, 2026
HCID 776593, compound → HCID 5201131, compound
https://huagongshe.com/reaction/2404945
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 776593 | HCID 776593 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 5201131 | HCID 5201131 | 72% |
Reaction Steps
8.00 g MnO2 (Activated, Fluka) was added to the suspension of 10 millimol VI in 60 milliliter toluene, and the suspension was stirred at reflux temperature for 5 days. The reaction mixture cooled down to 60° C., filtrated, and evaporated to give the desired compound VII as solid crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08802849B2 |
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| Source dataset | uspto-grants-2014_08 |
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| ORD ID | ord-cfa5549887b64b29b839b07c9fcc9444 |
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| Source note | uspto-grants-2014_08 |
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