HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Ethyl 2-amino-1-benzothiophene-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 5201131 | HCID 5201131 | — |
| Solvent | Methanesulfonic Acid | HCID 6395 | — |
| Product | Ethyl 2-amino-1-benzothiophene-3-carboxylate | HCID 699464 | — |
Reaction Steps
The solution of 10 millimol VII in 50 milliliter methanesulfonic acid was stirred at room temperature for 48 hours. The reaction mixture was poured onto icecold 25% aqueous NH3 solution, the soliw was filtered off, washed with water and n-hexane, then dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802849B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-5ec9d8affff240c1bfbbef12f8c50f13 |
| Source note | uspto-grants-2014_08 |