HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,3-Triethoxyprop-1-yne → HCID 22570286, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,3-Triethoxyprop-1-yne | HCID 10920972 | — |
| Reactant | 3-Bromo-5-(2,2,2-trifluoroethoxy)pyridine | HCID 22570352 | — |
| Product | HCID 22570286 | HCID 22570286 | 46% |
Reaction Steps
The title compound was synthesized from 3-bromo-5-(2,2,2-trifluoro-ethoxy)-pyridine and 3,3,3-triethoxypropyne using the procedure described in Example 43, step (e), in 46% yield. 1H NMR (CDCl3) δ 8.44 (bs, 1H), 8.35 (bs, 1H), 7.34 (m, 1H), 4.40 (q, 2H, J=7.9 Hz), 3.76 (q, 6H, J=7.1 Hz), 1.28 (t, 9H, J=7.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06855722B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-11e2f967ab0649b7be94a52068d1d18a |
| Source note | uspto-grants-2005_02 |