HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 3-Bromo-5-ethoxypyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3,5-Dibromopyridine | HCID 69369 | — |
| Product | 3-Bromo-5-ethoxypyridine | HCID 12293480 | 60% |
Reaction Steps
The title compound was synthesized from 3,5-dibromopyridine and ethanol using the procedure described in Example 53, step (a) in 60% yield. 1H NMR (CDCl3) δ 8.27 (bs, 1H), 8.23 (bs, 1H), 7.33 (m, 1H), 4.06 (q, 2H, J=7.0 Hz), 1.43 (t, 3H, J=7.0 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06855722B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-4c55b4c1142947ad8cbcf5785fb97f8f |
| Source note | uspto-grants-2005_02 |