Potassium Carbonate → HCID 11311797, compound

HRID 2405286Notes

Reaction equation

HRID 2405286 reaction equation
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, compound

Product 1

HCID 11311797HCID 11311797, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of step 1 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. After evaporation to dryness, the residue was used without further purification in the subsequent step.

Workup

  1. temperatureunder reflux
  2. customAfter evaporation to dryness
  3. customthe residue was used without further purification in the subsequent step

Sources & evidence

ORD record
ord-5e7102c7ccc84890af72a91870ac551a
Source dataset
uspto-grants-2014_08
Patent number
US08802720B2

Reaction notes

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