HRID240546

反应详情

EQUATION

反应方程式

HRID 240546 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 4-(benzyloxy)-2-chloropyridine (4.89 g, 22.30 mmol) in pyridine (120 mL) was added hydrazine (45 mL, 22.30 mmol). After heating to reflux for 18 hours, the mixture was concentrated to provide the crude product, which was used without further purification.

WORKUP

后处理

  1. temperatureAfter heating
  2. temperatureto reflux for 18 hours
  3. concentrationthe mixture was concentrated