HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 4-(Benzyloxy)-2-hydrazinylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 4-(Benzyloxy)-2-chloropyridine | HCID 53404197 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-(Benzyloxy)-2-hydrazinylpyridine | HCID 66937307 | — |
Reaction Steps
To a solution of 4-(benzyloxy)-2-chloropyridine (4.89 g, 22.30 mmol) in pyridine (120 mL) was added hydrazine (45 mL, 22.30 mmol). After heating to reflux for 18 hours, the mixture was concentrated to provide the crude product, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648087B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f6aa91d15140450d90740aa5fd3c2336 |
| Source note | uspto-grants-2014_02 |