HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-(Benzyloxy)-[1,2,4]triazolo[4,3-a]pyridine → HCID 178516347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-(Benzyloxy)-[1,2,4]triazolo[4,3-a]pyridine | HCID 66937047 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178516347 | HCID 178516347 | — |
Reaction Steps
To a solution of 7-(benzyloxy)-[1,2,4]triazolo[4,3-a]pyridine (0.512 g, 2.27 mmol) in ethanol (30 mL) was added Pd/C (0.5 g). After stirring under a hydrogen balloon for 3 hours, the mixture was filtered through celite and washed with ethanol (30 mL). The filtrate was concentrated under reduced pressure and chromatographed (20:1 dichloromethane/methanol) to provide the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648087B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-9687788a58914adfa5a8c4bbea2dd39b |
| Source note | uspto-grants-2014_02 |