HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 240554Generated: October 26, 2026
Dimethylformamide dimethyl acetal → HCID 178428760, compound
https://huagongshe.com/reaction/240554
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 4-(2-Methyl-4-nitrophenoxy)pyridin-2-amine | HCID 23153065 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178428760 | HCID 178428760 | — |
Reaction Steps
To a solution of 4-(2-methyl-4-nitrophenoxy)pyridin-2-amine (2.05 g, 8.34 mmol) in ethanol (9 mL) was added dimethoxy-N,N-dimethylmethanamine (1.18 mL, 8.34 mmol). After heating to 80° C. for 1 hour, the mixture was concentrated under reduced pressure to provide the crude product as dark oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08648087B2 |
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| Source dataset | uspto-grants-2014_02 |
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| ORD ID | ord-10476781d2334df78bb477caee31f24e |
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| Source note | uspto-grants-2014_02 |
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