HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethoxybenzaldehyde → HCID 68542497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethoxybenzaldehyde | HCID 70019 | — |
| Reactant | 1-(4-Bromophenyl)-2-(4-bromophenylthio)ethanone | HCID 43412626 | — |
| Product | HCID 68542497 | HCID 68542497 | — |
Reaction Steps
The title compound is prepared by the methods described in Synthesis Example 1. A solution of 1-(4-bromophenyl)-2-(4-bromophenylthio)ethanone (10 mmol) and 2,4,6-trimethoxybenzaldehyde (10 mmol) was subjected to the procedure described as Method B in part C of Synthesis Example 1 and the product obtained was purified by column chromatography. m.p 130-132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08808702B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-912c86346eea4038910917b2ec2c9163 |
| Source note | uspto-grants-2014_08 |