4-Bromobenzaldehyde → HCID 68540994, compound

HRID 2405542Notes

Reaction equation

HRID 2405542 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:18])[CH2:9][S:10][C:11]1[CH:16]=[CH:15][C:14]([Br:17])=[CH:13][CH:12]=1.[Br:19][C:20]1[CH:27]=[CH:26][C:23]([CH:24]=O)=[CH:22][CH:21]=1>>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:18])/[C:9](/[S:10][C:11]1[CH:16]=[CH:15][C:14]([Br:17])=[CH:13][CH:12]=1)=[CH:24]\[C:23]1[CH:26]=[CH:27][C:20]([Br:19])=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 707414-BromobenzaldehydeHCID 43412597HCID 43412597, compound

Product 1

HCID 68540994HCID 68540994, compound

Procedure

The title compound is prepared by the methods described in Synthesis Example 1. A solution of 1-(2-bromophenyl)-2-(4-bromophenylthio)ethanone (10 mmol) and 4-bromobenzaldehyde (10 mmol) was subjected to the procedure described as Method B in part C of Synthesis Example 1 and the product obtained was purified by column chromatography.

Workup

  1. customdescribed in Synthesis Example 1
  2. customdescribed as Method B in part C of Synthesis Example 1
  3. customthe product obtained
  4. customwas purified by column chromatography

Sources & evidence

ORD record
ord-406d0e78c8d64957a6785ecba9cf8221
Source dataset
uspto-grants-2014_08
Patent number
US08808702B2

Reaction notes

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