4-Bromobenzaldehyde → HCID 68539167, compound

HRID 2405544Notes

Reaction equation

HRID 2405544 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](=[O:19])[CH2:10][S:11][C:12]2[CH:17]=[CH:16][C:15]([Br:18])=[CH:14][CH:13]=2)=[CH:5][CH:4]=1.[Br:20][C:21]1[CH:28]=[CH:27][C:24]([CH:25]=O)=[CH:23][CH:22]=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:9](=[O:19])/[C:10](/[S:11][C:12]2[CH:13]=[CH:14][C:15]([Br:18])=[CH:16][CH:17]=2)=[CH:25]\[C:24]2[CH:27]=[CH:28][C:21]([Br:20])=[CH:22][CH:23]=2)=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 707414-BromobenzaldehydeHCID 43412616HCID 43412616, compound

Product 1

HCID 68539167HCID 68539167, compound

Procedure

The title compound is prepared by the methods described in Synthesis Example 1. A solution of 1-(4-methoxyphenyl)-2-(4-bromophenylthio)ethanone (10 mmol) and 4-bromobenzaldehyde (10 mmol) was subjected to the procedure described as Method B in part C of Synthesis Example 1 and the product obtained was purified by column chromatography.

Workup

  1. customdescribed in Synthesis Example 1
  2. customdescribed as Method B in part C of Synthesis Example 1
  3. customthe product obtained
  4. customwas purified by column chromatography

Sources & evidence

ORD record
ord-78849b3e16a9441d8472c5405f4f5758
Source dataset
uspto-grants-2014_08
Patent number
US08808702B2

Reaction notes

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