Tetramethyl orthocarbonate → HCID 68357450, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 500 mg of 1-(4-bromophenyl)-2-hydroxy-2-methylpropane-1-sulfonamide in 2 ml of tetramethoxymethane and 0.5 ml of acetic acid was stirred at 100° C. for 3 hours. After the removal of the solvent under reduced pressure, the residue (565 mg) was used in the next reaction without further purification.

Provenance & Evidence