2-Chlorophenol → 2-Chlorophenyl sulfamate

HRID 2405768Notes

Reaction equation

HRID 2405768 reaction equation
C1([O:4][S:5](=[O:8])(=[O:7])[NH2:6])CC1.[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[OH:16]>>[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[NH:6][S:5](=[O:8])(=[O:7])[O-:4].[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[O:16][S:5](=[O:7])(=[O:4])[NH2:6]

Participants

4

Reactant 2

HCID 72452-ChlorophenolHCID 57785190Cyclopropyl sulfamate

Product 2

HCID 216944982-Chlorophenyl sulfamateHCID 866327882-Chlorophenylsulfamate

Procedure

2-Chlorophenylsulfamate was synthesized according to the method presented in the synthesis of Sulfamic acid cyclopropyl ester in Example 1 with the exception of utilizing 2-chlorophenol to obtain sulfamic acid 2-chloro-phenyl ester.

Sources & evidence

ORD record
ord-a4e626f829e54610ae64eae0968de6d2
Source dataset
uspto-grants-2014_08
Patent number
US08809267B2

Reaction notes

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