Phenylsulfamate → Sulfamic acid 1-trifluoroethyl-cyclopropyl ester

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Phenylsulfamate	HCID 11030308	—
Edukt	1-(2,2,2-Trifluoroethyl)cyclopropan-1-ol	HCID 57445153	—
Produkt	Sulfamic acid 1-trifluoroethyl-cyclopropyl ester	HCID 57785491	—

Reaktionsschritte

Sulfamic acid 1-trifluoroethyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-trifluoroethylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-trifluoroethyl-cyclopropyl ester.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08809267B2
Quelldatensatz	uspto-grants-2014_08
ORD ID	ord-4d5f66587ce143d88f1a0a56ddffc01f
Quellennotiz	uspto-grants-2014_08