Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57704525 | HCID 57704525 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67419769 | HCID 67419769 | — |
Reaction Steps
Compound 21-7 (1.49 g) was dissolved in ethanol (20 ml), concentrated hydrochloric acid (3 ml) was added, and the mixture was stirred at 80° C. for 1.5 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (915 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08809304B2 |
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| Source dataset | uspto-grants-2014_08 |
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| ORD ID | ord-28620edbc043495cac1bc80e9300ebac |
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| Source note | uspto-grants-2014_08 |
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