HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-(2-Morpholinoethoxy)phenyl)butan-1-one → 1-(4-(2-Morpholinoethoxy)phenyl)butan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-(2-Morpholinoethoxy)phenyl)butan-1-one | HCID 66821978 | — |
| Reactant | HCID 66822143 | HCID 66822143 | — |
| Product | 1-(4-(2-Morpholinoethoxy)phenyl)butan-1-amine | HCID 66822028 | 70% |
Reaction Steps
The title compound was prepared by using a similar procedure as described for the preparation of 25 except that 1-(4-(2-morpholinoethoxy)phenyl)butan-1-one (24) was used instead of 1-(4-(2-(diethylamino)ethoxy)phenyl)butan-1-one (21). This produced crude 28 (390 mg, 70%) as a light yellow oil: MS (ES+) m/z 279.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809377B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-4e8b16aed365483ebb35b5009d3c7f78 |
| Source note | uspto-grants-2014_08 |