反应详情

The title compound was prepared by using a similar procedure as described for the preparation of 29 except that (S)-1-phenylbutylamine was used instead of 1-(4-(2-(diethylamino)ethoxy)phenyl)butan-1-amine (25). This produced crude product which was purified by flash silica gel column chromatography, eluting with 7:3 hexanes/ethyl acetate, to give 39 (375 mg, 58%) as a white solid: MS (ES+) m/z 217.1.1 (M+H)+.

1. customThe title compound was prepared
2. customThis produced crude product which
3. customwas purified by flash silica gel column chromatography
4. washeluting with 7:3 hexanes/ethyl acetate