HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-(5-methyl-hex-1-enyl)-1H-indole → 5-chloro-2-(5-methyl-hexyl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-(5-methyl-hex-1-enyl)-1H-indole | HCID 68751320 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-chloro-2-(5-methyl-hexyl)-1H-indole | HCID 68746927 | — |
Reaction Steps
5-Chloro-2-(5-methyl-hex-1-enyl)-1H-indole was dissolved in ethanol and 10% palladium on carbon was added to the solution. The reaction flask was sealed and exposed to hydrogen gas under pressure and was stirred for 5 hours. Then the reaction mixture was filtered through Celite. The solvent was evaporated to give 5-chloro-2-(5-methyl-hexyl)-1H-indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809382B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-6be766e0044a4a62bf3dd8814c8d9cc0 |
| Source note | uspto-grants-2014_08 |