Potassium Carbonate → HCID 66973877, compound

HRID 2406840Notes

Reaction equation

HRID 2406840 reaction equation
[OH:1][C:2]1[C:7]([CH2:8][CH2:9][CH3:10])=[CH:6][C:5]([O:11][CH3:12])=[C:4]([O:13][CH3:14])[CH:3]=1.Br[CH2:16][C:17]#[C:18][CH3:19].C(=O)([O-])[O-].[K+].[K+]>CC(C)=O>[CH2:16]([O:1][C:2]1[C:7]([CH2:8][CH2:9][CH3:10])=[CH:6][C:5]([O:11][CH3:12])=[C:4]([O:13][CH3:14])[CH:3]=1)[C:17]#[C:18][CH3:19]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 27568621-Bromo-2-butyneHCID 53143974,5-Dimethoxy-2-propylphenol

Product 1

HCID 66973877HCID 66973877, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Following the same procedure as in Example 7a) and 7b), 3.92 g (0.02 moles) of 1-hydroxy-6-propyl-3,4-dimethoxybenzene were reacted with 2.66 g (0.02 moles) of 1-bromo-2-butyne and 2.8 g (0.02 moles) of anhydrous potassium carbonate in 20 ml of acetone.

Sources & evidence

ORD record
ord-a8c85971451f4651bf9a538804f00076
Source dataset
uspto-grants-2014_08
Patent number
US08809389B2

Reaction notes

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