HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-6-(1-methylhydrazinyl)pyridazine → N'-(6-chloropyridazin-3-yl)-5-cyclopentyl-N'-methyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-6-(1-methylhydrazinyl)pyridazine | HCID 2735815 | — |
| Reactant | 5-Cyclopentyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid | HCID 71294186 | — |
| Product | N'-(6-chloropyridazin-3-yl)-5-cyclopentyl-N'-methyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide | HCID 71510017 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 1 using 5-cyclopentyl-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid (example 14c) and 3-chloro-6-(1-methylhydrazinyl)-pyridazine (CAN 76953-33-8) as starting materials; MS (EI) 430.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648099B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-865ea78e6f4f477fbe3e3d69dc9205ac |
| Source note | uspto-grants-2014_02 |