HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorophenylglyoxal hydrate → as-Triazine, 5-(2,4-difluorophenyl)-3-(methylthio)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorophenylglyoxal hydrate | HCID 2782300 | — |
| Reactant | Methyl hydrazinecarbimidothioate | HCID 178504051 | — |
| Product | as-Triazine, 5-(2,4-difluorophenyl)-3-(methylthio)- | HCID 3053040 | 78% |
Reaction Steps
3-(Methylsulfanyl)-5-(2,4-difluorophenyl)-1,2,4-triazine (1.00 g, 78%) was prepared from methyl hydrazinecarbimidothioate (0.63 g, 6.0 mmol) and 2,4-difluorophenylglyoxal monohydrate (1.00 g, 6.0 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-19e9a95df52b4444833f118177382581 |
| Source note | uspto-grants-2014_08 |