HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methoxymethyl)phenylglyoxal → 5-[4-(Methoxymethyl)phenyl]-3-(methylsulfanyl)-1,2,4-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methoxymethyl)phenylglyoxal | HCID 54306153 | — |
| Reactant | Methyl hydrazinecarbimidothioate | HCID 178504051 | — |
| Product | 5-[4-(Methoxymethyl)phenyl]-3-(methylsulfanyl)-1,2,4-triazine | HCID 67364981 | 72% |
Reaction Steps
5-[4-(methoxymethyl)phenyl]-3-(methylsulfanyl)-1,2,4-triazine (4.0 g, 72%) was prepared from methyl hydrazinecarbimidothioate (7.33 g, 31.46 mmol) and 4-(methoxymethyl)phenylglyoxal (4 g, 22.47 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-bea97205bb2d49ef8a3f7a9563b44814 |
| Source note | uspto-grants-2014_08 |