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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2407089Generated: October 30, 2026

146535-00-4 → HCID 67365291, compound

https://huagongshe.com/reaction/2407089

Reaction equation

Participants

RoleNameHCIDCharge
Reactant146535-00-4HCID 18784701—
ReactantMethyl hydrazinecarbimidothioateHCID 178504051—
ProductHCID 67365291HCID 6736529180%

Reaction Steps

3-(methylsulfanyl)-5-(3,5-difluorophenyl)-1,2,4-triazine (28 g, 80.0%) was prepared from methyl hydrazine carbimidothioate (20.68 g, 197.4 mmol) and 2-(3,5-difluorophenyl)-2-oxoacetaldehyde (25 g, 147.0 mmol) according to the general procedure of Preparation 2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08809525B2
Source datasetuspto-grants-2014_08
ORD IDord-abb464f8b92d43a282bb3435d245e5c4
Source noteuspto-grants-2014_08