HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methoxyphenylboronic acid → 6-(5-Chloro-2-methoxyphenyl)-5-phenyl-1,2,4-triazin-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methoxyphenylboronic acid | HCID 2735751 | — |
| Reactant | 6-Bromo-5-phenyl-1,2,4-triazin-3-amine | HCID 86676114 | — |
| Product | 6-(5-Chloro-2-methoxyphenyl)-5-phenyl-1,2,4-triazin-3-amine | HCID 53354523 | 22.8% |
Reaction Steps
6-(5-Chloro-2-methoxyphenyl)-5-phenyl-1,2,4-triazin-3-amine (57 mg, 22%) was prepared from 6-bromo-5-phenyl-1,2,4-triazin-3-amine (0.21 g, 0.80 mmol) and 5-chloro-2-methoxyphenylboronic acid (0.15 g, 0.80 mmol) according to the general procedure of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-985847a93c444ce581dd66d497e6e47a |
| Source note | uspto-grants-2014_08 |