HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Ethynylpiperidine hydrochloride → 6-(3-Ethynylpiperidin-1-yl)-5-phenyl-1,2,4-triazin-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Ethynylpiperidine hydrochloride | HCID 53401123 | — |
| Reactant | 6-Bromo-5-phenyl-1,2,4-triazin-3-amine | HCID 86676114 | — |
| Product | 6-(3-Ethynylpiperidin-1-yl)-5-phenyl-1,2,4-triazin-3-amine | HCID 53353904 | 2% |
Reaction Steps
6-(3-Ethynylpiperidin-1-yl)-5-phenyl-1,2,4-triazin-3-amine (10 mg, 2%) was prepared from 6-bromo-5-phenyl-1,2,4-triazin-3-amine (0.60 g, 2.40 mmol) and 3-ethynyl piperidine HCl (0.42 g, 2.87 mmol) according to the general procedure of Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809525B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-a339a2df046046309a77c0a5dbbc14c3 |
| Source note | uspto-grants-2014_08 |