HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-(N-Pyrimidin-2-ylhydrazino)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloropyrimidine | HCID 74404 | — |
| Reactant | Hydrazinoethanol | HCID 19013750 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(N-Pyrimidin-2-ylhydrazino)ethanol | HCID 58416028 | — |
Reaction Steps
4.8 g (41.9 mmol) of 2-chloropyrimidine in 100 ml of ethanol and 3.6 g (47 mmol) of hydrazinoethanol and 9 g (64.2 mmol) of potassium carbonate were heated under reflux for 5 h. The mixture was filtered off with suction and the filtrate was concentrated by evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809547B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-7780fa72642443dd9b1df9a28bc8889e |
| Source note | uspto-grants-2014_08 |