HRID2407387

反应详情

EQUATION

反应方程式

HRID 2407387 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4.8 g (41.9 mmol) of 2-chloropyrimidine in 100 ml of ethanol and 3.6 g (47 mmol) of hydrazinoethanol and 9 g (64.2 mmol) of potassium carbonate were heated under reflux for 5 h. The mixture was filtered off with suction and the filtrate was concentrated by evaporation.

WORKUP

后处理

  1. temperatureunder reflux for 5 h
  2. filtrationThe mixture was filtered off with suction
  3. concentrationthe filtrate was concentrated by evaporation