HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 53868659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Cyclohexanesulfonyl chloride | HCID 237554 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53868659 | HCID 53868659 | — |
Reaction Steps
To a stirred solution of 2-phenylethylamine (0.60 g, 4.97 mmol) in 45 ml CH2Cl2 at room temperature was added Et3N (0.83 ml, 5.97 mmol). The mixture was stirred for 5 min, and then cyclohexanesulfonyl chloride (1.0 g, 5.47 mmol) was added at this temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809584B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-383e9e9503ac43b2b597456d96a7b874 |
| Source note | uspto-grants-2014_08 |