Hydrochloric Acid → HCID 66989815, compound

Participants

Reaction Steps

The compound prepared in Example 76 (0.05 g) was suspended in 1,4-dioxane (4 mL), hydrochloric acid (4 mol/L solution in 1,4-dioxane, 0.88 mL) was added and the reaction mixture was stirred at room temperature overnight. The reaction mixture was concentrated to obtain the title compound (0.04 g) having the following physical data.

Provenance & Evidence