HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86659057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58503919 | HCID 58503919 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86659057 | HCID 86659057 | — |
Reaction Steps
A solution of the compound prepared in Example 159 (100 mg) in dichloromethane (1 mL)-trifluoroacetic acid (228 mL) was stirred for 30 minutes. The reaction was concentrated and the excess trifluoroacetic acid was removed via azeotropic distillation from toluene and hexane to obtain the title compound (110 mg) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809538B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-3c713ea185de478fa58bc9e33b617008 |
| Source note | uspto-grants-2014_08 |