HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66989693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86659059 | HCID 86659059 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66989693 | HCID 66989693 | — |
Reaction Steps
A solution of the compound prepared in Example 243 (0.088 g) in dichloromethane (1 mL) was treated with 4N hydrogen chloride in dioxane (0.151 mL) at room temperature. The mixture was stirred at room temperature for 18 hours. The solvent was evaporated in vacuo to provide the title compound (0.072 g) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08809538B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-28b8c455a42e41f98b01939d3dce6c80 |
| Source note | uspto-grants-2014_08 |