HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2407848Generated: November 1, 2026
Triethyl Phosphate → HCID 15260324, compound
https://huagongshe.com/reaction/2407848
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl Phosphate | HCID 6535 | — |
| Reactant | Bis(2-bromoethyl) ether | HCID 21521 | — |
| Product | HCID 15260324 | HCID 15260324 | — |
Reaction Steps
1-bromo-2-(2-bromoethoxy) ethane (1.0 eq) was mixed with triethyl phosphate (1 eq) then heated to 160° C. for 20 minutes by microwave. The crude mixture was purified by flash chromatography on a COMBIFLASH® system (ISCO) using 70-100% EtOAc/Hex to give the product as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08808703B2 |
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| Source dataset | uspto-grants-2014_08 |
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| ORD ID | ord-473483d66c544ce0811ca5fd9ff78dae |
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| Source note | uspto-grants-2014_08 |
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