HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perfluoro-2-methyl-3-oxahexanoic acid → HCID 86682209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perfluoro-2-methyl-3-oxahexanoic acid | HCID 114481 | — |
| Reactant | (4-tert-Butylphenyl)(diphenyl)sulfanium bromide | HCID 22625536 | — |
| Product | HCID 86682209 | HCID 86682209 | 37% |
Reaction Steps
Synthesis was carried out as in Synthesis Example 1 aside from using 13.2 g (0.04 mol) of 2,3,3,3-tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)propionic acid and an amount (0.06 mol) of 4-tert-butylphenyldiphenylsulfonium bromide aqueous solution. There was obtained 9.5 g of white crystals (yield 37%). The compound thus obtained was analyzed by spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815492B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-a1af19734bc943158aed61846e49df35 |
| Source note | uspto-grants-2014_08 |