HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 68034535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | 1-Aminocyclopentanemethanamine | HCID 199818 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68034535 | HCID 68034535 | 138.8% |
Reaction Steps
3.35 g of 1-(aminomethyl)cyclopentanamine are solubilized in 20 mL of water, cooled beforehand in an ice bath. 3.52 g of BrCN are added and the mixture is then stirred for 3 h at RT. The solvent is evaporated. 5.67 g (yield=88%) of 1,3-diazaspiro[4.4]non-2-en-2-amine are obtained as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815853B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-c74b8b6268b8439d84098a1b63101773 |
| Source note | uspto-grants-2014_08 |