HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 58993735, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 4-(4-Aminophenyl)cyclohexan-1-one | HCID 23371894 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58993735 | HCID 58993735 | — |
Reaction Steps
The title compound was prepared from 4-(4-amino-phenyl)-cyclohexanone (as prepared in the previous step) by bromination with NBS according to the procedure in Example 4, step (b), replacing CH3CN with CH2Cl2. Mass spectrum (ESI, m/z): Calcd. for C12H14NOBr, 268.0/270.0 (M+H), found 268.3/270.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815867B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-614b6c5c8337435f888047575650cc11 |
| Source note | uspto-grants-2014_08 |