HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 50991730, compound → HCID 50991731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 50991730 | HCID 50991730 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 50991731 | HCID 50991731 | — |
Reaction Steps
Methanol (2 mL) was added to 4-(6-(3-nitrophenyl)-1-(pyridin-4-yl)-1H-indol-3-yl)phenol (4.6 mg, 0.0113 mmol) and 10% (w/w) palladium-carbon (Pd—C, 5.0 mg). The mixture was stirred at room temperature for 12 hours under hydrogen gas (1 atm). The reaction solution was filtered using a diatomite pad and concentrated under reduced pressure. The target compound was obtained as brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648089B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-79b912f6b90e4bbfaaaacb034909eac0 |
| Source note | uspto-grants-2014_02 |