HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67386428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | tert-Butyl 7-benzyl-2,7-diazaspiro[3.5]nonane-2-carboxylate | HCID 45790087 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67386428 | HCID 67386428 | — |
Reaction Steps
To a solution of tert-butyl 7-benzyl-2,7-diazaspiro[3.5]nonane-2-carboxylate (CAS 929301-99-5 WO2007030061) in methanol was added 4 N HCl/dioxane. The mixture was stirred at room temperature for 2 hours. The reaction mixture was then concentrated to obtain the title compound. MS (DCI+) m/z 217 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815869B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-0931c84e8efb420395ec0559a98c4c80 |
| Source note | uspto-grants-2014_08 |