HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Fluoro-phenyl)-piperidine hydrochloride → HCID 53377694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Fluoro-phenyl)-piperidine hydrochloride | HCID 21898168 | — |
| Reactant | HCID 71178961 | HCID 71178961 | — |
| Product | HCID 53377694 | HCID 53377694 | 14.9% |
Reaction Steps
Using ethyl 3-(N-cyclopropylsulfamoyl)-7-(4-fluoro-2-methylphenylamino)-pyrazolo[1,5-a]pyrimidine-6-carboxylate (0.496 g, 1.145 mmol) obtained in step 1 and 4-(4-fluorophenyl)piperidine hydrochloride (0.072 g, 0.335 mmol) instead of 4-phenylpiperidine, and in the same manner as in Example 1 step 4, the title compound (0.0283 g, 3%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-7ed72e8ec4f249748b1c7bc59e905626 |
| Source note | uspto-grants-2014_08 |